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Title: Cyclophanes, XLIV synthesis of 4,5,12,13-tetraformyl[2.2]paracyclophane and its bis-acetal
Authors: Sankararaman, S.
Hopf, H.
Dix, I.
Jones, P.G.
Keywords: acetal derivative
aldehyde derivative
paracyclophane derivative
chemical analysis
chemical structure
crystal structure
structure analysis
X ray crystallography
Issue Date: 2000
Citation: European Journal of Organic Chemistry, (15), 2699-2701
Abstract: 4,5,12,13-Tetraformyl[2.2]paracyclophane (1f) has been prepared for the first time by the cycloaddition of 4,4-diethoxy-2-butynal (3) to 1,2,4,5-hexatetraene (2) under various conditions and hydrolysis of the initially produced bis-acetals 5a and 5b. An X-ray crystal structural analysis of 5a is reported.
ISSN: 1434193X
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