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|Title:||Cyclophanes, XLIV synthesis of 4,5,12,13-tetraformyl[2.2]paracyclophane and its bis-acetal|
X ray crystallography
|Citation:||European Journal of Organic Chemistry, (15), 2699-2701|
|Abstract:||4,5,12,13-Tetraformyl[2.2]paracyclophane (1f) has been prepared for the first time by the cycloaddition of 4,4-diethoxy-2-butynal (3) to 1,2,4,5-hexatetraene (2) under various conditions and hydrolysis of the initially produced bis-acetals 5a and 5b. An X-ray crystal structural analysis of 5a is reported.|
|Appears in Collections:||Articles|
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