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I <inf>2</inf>-TEMPO as an efficient oxidizing agent for the one-pot conversion of alcohol to amide using FeCl <inf>3</inf> as the catalyst

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05-09-2012
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Research Projects
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Abstract
A high yield one-pot method for the synthesis of amides from alcohols is described. The aldehyde was generated in situ using iodine-TEMPO as oxidizing agent followed by intermediate oxime formation through reaction with NH 2OH•HCl and finally rearrangement of oxime catalyzed by FeCl 3. © 2012 Elsevier B.V. All rights reserved.
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Alcohol, Amide, Catalyst, FeCl 3, I -TEMPO 2
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